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Core Facilities and Service Group

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Core Facility

Imaging of Materials Systems

  • The 3D visualization of complex functional and adaptive (micro)systems in biology and technology is one of the central challenges in basic research on adaptive and bio-inspired technologies and in the investigation of functional principles in biological systems as a source of ideas for new technical developments.
  • Using existing and newly acquired equipment, it is possible to establish a specialized laboratory for microscopy and tomography of materials combined with an FIT competence network for 3D visualization.
  • If you have any further questions regarding the costs (fee regulation), usage regulations and registration procedure, please contact the management of the Core Facility.
  • Scientific Head: Prof. Dr. Anna Fischer
  • Responsible Manager: Dr. Yi Thomann

Equipment

Talos 200X - HRTEM/HRSTEM

Talos 200X – HRTEM/HRSTEM

  • 200 kV high-brightness X-FEG
  • Modes: TEM, STEM, HAAFD, DF, DPC
  • SuperX EDX System
  • (limited) Cryo TEM, STEM
  • TEM Holder: Double Tilt, High Tilt, Cryo
  • Piezo-Stage 20 pm
  • Low-dose technique
  • Ceta 16 Megapixel Digital Camera
  • Auto tilt series imaging
  • Tomography reconstruction
  • Application areas:
  • Solid state inorganic and soft matter materials (metals, semiconductors, composites, polymers etc).
  • 2D (up to atomic resolution) and 3D imaging.
  • 2D EDX analytics (point analysis and mapping).
120 kV TEM: Talos L120C G2

Talos 120C – TEM

  • 120 kV LaB6 gun
  • Double Tilt, High Tilt and Cryo Holders
  • Ceta 16 Megapixel Camera
  • Auto tilt series imaging
  • Tomography reconstruction
  • Low-dose technique
  • Application areas:
  • TEM and Cryo TEM of soft matter samples, Cryo TEM Tomography
FIB/SEM Anlage: Scios2

Scios 2 HiVac – Focused Ion Beam / Scanning Electron Microscopy

  • 30 kV FEG
  • Gallium-ion-column
  • SE, T1, T2 and DBS Detektors
  • C and Platin deposition
  • Tomography equipment
  • EDAX EDX System
  • Mikromanipulator
  • PraparationPreparation of TEM Lamella
  • Auto slice and view (ASNV)
  • Avizo
  • Application areas:
  • SEM imaging, FIB micro/nanostructuring, EDX analysis (point and map analysis), FIB-SEM Tomography, TEM lamellae preparation
SKYSCAN 1272 - µCT

SKYSCAN 1272 – µCT

  • X-ray source: 20-100 kV, 10 W, <5 μm spot size @ 4 W
  • X-ray detector: 16 Mp, 14-bit cooled CCD fiber-optically coupled to scintillator
  • Maximum object size 75 mm in diameter using offset scan (27 mm in fast single scan)
  • Detail detectability 0.35 μm (16 Mp) at highest magnification
MultiMode 8 with Nanoscope V - AFM

MultiMode 8 with Nanoscope V – AFM

  • Contact and Tapping Modes, phase imaging, Nanoindentation etc.
  • Resolution up to 0.1 nm, image range maximum 100 µm, depth maximum 2 µm;
  • Main applications: Studies on the crystallization behavior of polymers, polymer blends, block copolymers as well as surfaces of metals, semi-metals, nanocomposites etc.; not only surface but also bulk investigations of the samples by microtomy can be carried out.
Vitrobot Mark IV - Vitrification Robot

Vitrobot Mark IV – Vitrification Robot

  • PC-controlled device for vitrification (rapid cooling) of aqueous samples
  • Optimized for ethane and/or propane as coolants
  • Ultrasonically controlled humidification, optimized for operation at 90% – 100% RH; Peltier controlled heating/cooling; chamber temperature 4 – 60 °C
  • Automated lift and transfer of the coolant container
  • Cryo grids storage box and holder; semi-automated grid transfer
EM ICE with AFS 2 and AF - High Pressure Freezer with Freeze Substitution and Low Temperature Embedding System

EM ICE with AFS 2 and AF – High Pressure Freezer with Freeze Substitution and Low Temperature Embedding System

  • Vitrification of aqueous samples at a pressure of 200 MPa
  • Automatic process
  • Freeze substitution
  • Automatic dosing and embedding
  • Light stimulation